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Heck CouplingBTC [bis(trichloromethyl)carbonate] or POCl3 to yield the intermediate, immonium chlorides, which were subsequently reacted with the corresponding hydroxyl. Gilon has recently reported the use of BTC (Fig. 20) as a chlorinating reagent in solid-phase peptide synthesis Coupling reactions mediated by BTC gave good. A novel, highly efficient and racemization free coupling procedure for sterically hindered N-alkyl amino acids has been developed using triphosgene and a.